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Beilstein J. Org. Chem. 2013, 9, 754–760, doi:10.3762/bjoc.9.85
Graphical Abstract
Scheme 1: Phenylnitrene–2-pyridylcarbene rearrangement.
Scheme 2: Type I and type II ring opening and ring expansion in 3- and 2-pyridylnitrenes, respectively.
Scheme 3: FVT reactions of 4-azidopyridine (18), 2-(5-tetrazolyl)pyrazine (23) and triazolo[1,5-a]pyrazine (24...
Figure 1: Difference-IR spectrum of 2-diazomethylpyrazine (22) (positive peaks) in Ar matrix at 7 K, obtained...
Figure 2: Ar matrix IR-difference spectra showing the products of broadband UV photolysis of 4-azidopyridine (...
Figure 3: Top: calculated IR spectrum of 20 at the B3LYP/6-31G* level (wavenumbers scaled by 0.9613): ν’ (rel...
Figure 4: Bottom: IR spectrum from the matrix photolysis of azide 18 after the azide has been depleted comple...
Scheme 4: Photolysis reactions of azide 18 and triazole 24 in Ar matrix.